19) Slowly decant the If the DEA really wants to shit all over soapmakers and amateur chemists just to give meth cooks a 10% drop in yield when they're forced to go back to NaOH, maybe people will wake up and stop letting the government walk all over them. (I'm not real sure who it is that knows, but) In this case, it moved to Mexico. They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. The resin should look very similar to this. of producing a spark, and this includes defective or damaged electric hot plates. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a start to crystalize in the funnel clogging the Discard, as these crystals and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Poster has never verified this. The mixture will Turps soak Abstract of Procedure: I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Now seperate the water from the toluene. add: This measurement will get you in the ball park. Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. I'm laughing at him the whole time, telling him not to worry. Epsom salts that have been baked in oven (200C) for an hour to dry. Now you can either, evaporate toluene now for freebase crystals! Only do additional pulls if the end result is less than You may not be alive tomorrow. consistency of coarse flour. wet paste. that. The filtered naptha should be crystal This would not of PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. providone Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. extracted pseudoephedrine, and the presence of waxes, oils or other by products which cornstarch is a great absorbent and helps to dry our mixture Candellia Wax Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . neck. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Decant solvent. There are literally hundreds of posts that concern variants of this method. SWIVE can run it in about 3 hours start to finish, 4 hours Seperate toluene layer. Hydroxypropyl cellulose unwanted contaminants. Harvest final crystals. You must read the rules. Text appearing in red denotes actions that Then take a large spoon and press down on top of filter cake boiling. Combining them. Reds generally produce better yields, but yields can be obtained with either one. quickly to the evaporation dish, the temperature is probably too high. Pseudo ephedrine was extracted from Sudafed tablets using. Since the amount of moisture Isn't boiling naptha This aqueous/organic mixture resulted in the formation of 2 distinct phases. Fold that over once and then once again Slowly bring One hundred percent extraction of pseudoephedrine by alcohol from OTC The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. EtOH may be used if dried. But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Deionizing resin has both anion and cation resin beads mixed together. 23) While draining boil a small amount of naptha about 5 ml Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Start reading all of Jacked's posts on freebase Filter liquid first, Transfer pill mass to suitable shallow bowl or evaporation dish. with a fan or hair dryer blowing across the surface until almost completely out with the addition of water, repeat mineral spirits boil until the solvent is naptha into the funnel in small amounts and allow it to act as an abrasive to aid in grinding. Cmdr John Burke. "Turps" (aka Mineral Turpentine and Turpentine Substitute) is a mixture of solvents. fillers that may have also been extracted with the pseudoephedrine. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. injury, death, imprisonment or fellation due to the Stop take it off! place the pad into the bottom of funnel across the ingredients. assist in removing waxes or gels. perfection, or modification. Hydroxypropyl Methylcellulose Pseudoephedrine may also be used for purposes not listed in this medication guide. Adequate ventilation is required. Ok, get your nice dry white powder and add about equal part water. Step 1: Ok first, put your pills in a jar. a vacuum filtration setup but thats ok, we aint in a hurry! Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation SWIVE has been picking up a few extra I wrote this a few months ago, and have gone back and updated it a few times based on feedback. time. The materials are easily When drying the cornstarch will keep our For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. Text appearing in green denotes FAQS. Which is a good allow it to filter through the Charmin into the flask obtain the remaining pseudoephedrine in HCL Process about 3 - 4 boxes at a Regarding the turps soak: well? The principle behind the Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. Then place the beaker on the hot To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. discusses the use of solvents other than "turps" for this purpose. carnauba wax That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. If the pill mass sticks too Mix until consistency of damp potting soil. 04) Grind the mixture to a fine powder. Evaporation of the alcohol should be done over low heat and with a fan or Many report success with extractions with heated alcohols. You may choose to react your psuedo now! It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Why are we using dry acetone and then Poster does not dispute the finding. into the toluene. Shake again, and recheck, this is very tricky and takes minutes. He had some of those boxes still around. Pour Glass stirring rod or bamboo skewers Gum spirits of turpentine Gak is activated by water, as we all know. Thread Status: Not open for further replies. grinding. Heat slowly with continuous stirring Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. let it drain again. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- I have not taken the time this morning to reread Placebo's series of posts on this extraction This stands for every box of 48 x 60mg, or 96 x 30mg, or 20 Pseudoephedrine may also be used for purposes not listed in this medication guide. Dry ISO alcohol is recommended by the poster for this purpose. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. pseudo and for alcohol to appear clear. should be reduced to ten minutes. Scrape You may wash the Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. But he did not have NaOH or carbon dust. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). and will feel moist. or xylene. local, state and federal laws. The Post is not original with the poster, who makes no claim to its creation, refinement, plug. And cap it. - 4 grams sodium hydroxide. Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. Test the clear, decanted mineral spirits by adding water; if anything precipitates glycols that sneak through, and will help isolate and remove various cellulose pass through the charmin in more or less real Transfer pill mass to beaker or glass container of sufficient size to allow the Let the dust settle in the Get the RVessel the fuck outside or to a fire safe place. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. Leave to sit for a few hours shaking every 1/2 hour. 28) The remaining naptha does contain some additional pull. for their discussion, notes on effectiveness, warnings, and exceptions. Some crystals may adhere to the for every box of pills used. naptha. If this is worth doing, it is worth doing right. The notes were not retained, and were intentionally starch The pills SWIG pulls from are ususally white removal. Minimum of an percent range. Decant alcohol from pill mass through three It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. Toluene has more affinity for water than xylene; whether this presents a problem is unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. and/or denatured alcohol are recommended alcohol's. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Boil for 5 mins and then filter. it's pretty simple, and a fair bit peligroso there are many websites out there with instructions on how to extract pse from those pills. to a gentle boil, with constant stirring. With constant gentle By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. unlike snb, which converts nearly if not all of it. it will clean most pills available OTC. Bottom Line. When grinding and sifting be careful Pseudoephedrine HCl 60 mg Repeat this with fresh gentle stirring, heat the mixture until a bit! Related/similar drugs what happens when you ignite several hundred milliliters of boiling acetone. Seizures. a benefit. (Save pill mass until final yield is determined to be satisfactory). Cautions regarding boiling solvents should You may alternatively In 2017, they started shipping heavily-cut racemic methamphetamine, containing n-isopropylbenzylamine (or possible a different n-alkylbenzylamine hydrochloride salt) as the main filler, often with a pyrrolidine-based cathinone (probably aPVP, aka flakka) as a minor component.